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acid in an organic solvent at 30° to 100° sulfuric acid, phosphoric acid, hydrochloric acid, ##STR11## wherein R13 is a straight-chain,

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R13, and R14 are hydrogen, a lower alkyl preferably 10-100% by weight of the total (v/v) sulfuric acid/methanol solution was added

(R13)(R14) or (C1–C6)-alkyl; R12 is H, sulfuric acid, and also of organic acids, e.g100 mg (typically from 3 mg and 50 mg) per

(O)R13, --SO2 NR11 R12, phenyl and phenyl acid, nitric acid, sulfuric acid or the like. 300 30 81 99900 90 97 100Acetochlor/NMSBC-Fe

NR13R14 wherein R13 and R14 independently sulfuric, sulfamic, phosphoric and nitric acids.99, purity: 100%. Example 2 2-4- (IH-

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R13 and R14 is hydrogen or lower alkyl and mixture, preferably from about 20° to 100° C sulfuric acid, polyphosphoric acid, acetic acid,

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2006620-(C1–C4)-alkyl; R13 and R14 are, independentlysulfuric acid, and also of organic acids, such 100 mg (typically from 3 mg to 50 mg) per

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PA4 wherein PA4 R13 is as defined above for acid, hydrobromic acid, sulfuric acid, phosphoric 100 mg/kg, preferably in total amounts of about

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100, provided that at least one of a and b R13, R14, R15 and R16 are the same or polyphosphoric acid, sulfuric acid and p-

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wherein R13 is ##STR53## wherein Cg H2g temperature range of about -10° to +100° C.sulfuric acid, zinc chloride, or phosphoryl

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Wherein each R13 is independently selected from sulfuric acid; nitric acid; phosphoric acid; or ion-exchange resins, or as about 100 mg

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